Chromatography and Separation Techniques- Partitioning of Iodine in Solution

Partitioning of Iodine in Solution

Description: Equimolar solutions of iodine in both hexane and water are shaken in a separatory funnel with either water or hexane. The iodine in water is driven to the hexane layer, but not visa versa, as seen by the color of iodine.

Source: UW Card Catalog

Year: N/A   Vol: N/A   Page: N/A

Keywords: Mineral Oil, Water, Hexane, Iodine

Rating:

Hazard: High

  • Acute toxicity hazard – inhalation, dermal, oral
  • Flammability hazard
  • Acute and chronic aquatic toxicity hazard
  • Aspiration hazard
  • Skin irritation
  • Eye irritation
  • Reproductive toxicity
  • Specific organ toxicity – central nervous system, respiratory system, thyroid

Effectiveness: Good

  • Results are clearly observable without guidance
  • Time to results is low
  • Good connection from demo to course material
  • Mild effects are seen are by audience
  • Good reliability

Difficulty: High

  • Complex lab equipment manipulations
  • Use of toxic and flammable compounds
  • Requires training or extended practice to perform correctly
  • Handle lab equipment with care
  • Procedures with multiple steps
  • Requires deep attention

Safety Precautions:

  • Gloves required
  • Eye protection required
  • Perform in a well-ventilated area
  • ABC fire extinguisher on hand
  • Perform on chemically resistant surface
  • Prior training required
  • Absorbent material on hand
  • Prevent release of reagents to the environment

 

Class: Equilibrium, Organic Chemistry, Phase Solubility

Division: General, Organic Chemistry, Analytical Chemistry

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